Biomedical Engineering Reference
In-Depth Information
R
4
NH
2
Yield (%)
b
Entry
Amine
Product
5
35e
,76
6
35f
,60
7
35g
,50
8
35h
,68
a
Reaction conditions: (
30a
red
)
=
2 mM, amine,
31
=
R
4
NH
2
=
20 mM, MeOH, rt, Hg anode (
E
=+
50 mV vs. SCE), 6 to 10 h.
b
Yields refer to chromatographically pure isolated products.
c
Obtained as a mixture of two unassigned diastereoisomers (ca. 1 : 1 ratio).
