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Fig. 12 Block diagram of the reactor
jackets ensure the circulation of a coolant
fl
fluid which is intended for heating or
for cooling the reactor.
￿
A heat exchanger: It allows to heat or to cool the coolant
fluid circulating
through the reactor jacket. Heating is carried out by three electrical resistances
controlled by a dimmer for varying the heating power. It is intended to achieve
the required reaction temperature of the esteri
fl
cation. Cooling is provided by
circulating cold water through the heat exchanger. It is used to cool the reactor
when the reaction is completed.
A condenser: It allows to condense the steam generated during the reaction. It
plays an important role because it is also used to indicate the end of the reaction
which can be deduced when no more water is dripping out of the condenser.
￿
A data acquisition card between the reactor and the calculator.
￿
The ester production by this reactor is based on three main steps as illustrated in
Fig. 13 .
Fig. 13 Specific trajectory of
the reactor temperature
100
Cooling
stage
Reacting
stage
Heating
Stage
0
300
540
Time(min)
 
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