NMR of Membrane Proteins - Recent Developments in Biomolecular NMR - page 288

Figure 12.3 Comparison of [ 15 N, 1 H] TROSY spectra and 1D translational diffusion

data for pSRII in different membrane mimics: (a) 0.5 mM pSRII in 2.4%
c7-DHPC, 800 MHz, 323 K, 32 scans; (b) 0.3 mM pSRII in 1.5% DDM,
800 MHz, 333 K, 32 scans; (c) 0.45 mM pSRII, 3.6% HEGA-10, 600
MHz, 323 K, 40 scans; (d) 0.45 mM pSRII, 5% NG, 600 MHz, 323 K,
32 scans; (e) 0.45 mM pSRII in q 5 0.4 DMPC/c7-DHPC bicelles, 800
MHz, 308 K, 1320 scans; (f) 0.45 mM pSRII in q 5 0.25 DMPC/c7-
DHPC bicelles, 800 MHz, 308 K, 480 scans; (g) Translational diffusion
at different temperatures recorded using the BPP-LED sequence (see
text) at 500 MHz.