Biomedical Engineering Reference
In-Depth Information
a
100
90
80
70
60
50
40
30
20
10
0
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
Time (min)
b
100
90
80
70
60
50
40
30
20
10
0
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
Time (min)
-CONHCH
2
CH
3
+H
c
150.0
100
44.0
NHCH
2
CH
3
90
193.0
O
-CH
2
CH
3
+H
N
80
107.0
70
60
N
149.0
-NHCH
2
CH
3
-NHCH
2
CH
3
50
78.0
177.0
-CH
3
40
151.0
O
O
N
77.0
105.0
30
206.0
NH
HN
133.0
20
104.0
17
8.0
51.0
5
2
.1
5
3
.0
72.0
164.0
93.0
122.0
221.0
10
42
.1
80.0
22
2.1
248.1
275.6 289.1
0
40
60
80
100
120
140
160
180
200
220
240
260
280
m/z
Figure 9.3. Solvent-extractable product formed from Cu:PDTC in the presence of ethylamine.
(a) GC chromatogram of extract from reaction mixture including ethylamine and Cu:PDTC.
(b) chromatogram of extract from reaction mixture including ethylamine, Cu:PDTC and CCl
4
.
(c) EI mass spectrum of peak eluting at 10.35 min in b.
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