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Scheme 2 Iron( III ) chloride debenzylations. Phth = Phthaloyl.
OH
OH
H 2 SO 4
O
O
H HO
H HO
MeOH
OH OH
OH OMe
8
9
8
10
D -glucose
D -galactose
FeCl 3 (1 equiv)
MeOH
rt
60 °C
HO
HO
O
HO
OH O
OMe
OMe
HO
OH
OH
HO
11
12
, 75%
, 75%
Scheme 3 Fischer glycosylation and Lubineau-Fischer ferric chloride version.
quite challenging for the one-step chemical synthesis of glycosides when
the amount of the nucleophile is limited. 17 A century later, Andr´
Lubineau and Jean-Claude Fischer replaced the protic acid by a Lewis acid. 18
Strikingly, treatment of D -glucose and D -galactose with ferric chloride
(1 equiv) in methanol at room temperature ( D -glucose) or 60 1C( D -galac-
tose) gave the corresponding methyl D -furanosides 11 and 12 in 75% yield,
instead of the thermodynamically more stable pyranosides (Scheme 3).
Iron( III )-sugar complexes apparently prevent ring expansion to the
more stable anomers. This one-step preparation of furanosides from the
unprotected hexoses was instrumental in the development of synthetic
routes leading to important bio-relevant targets. Some representative
reports that rely on the use of this unique transformation are presented
below. First, Plusquellec and co-workers modified this version to a
practical glycosylation using only 1.5 equiv of simple alcohols in THF or
1,4-dioxane as solvents with D -glucose, D -galactose, D -mannose and
D -galacturonic acid (Scheme 4). 19
Currently this reaction is often the starting point in the multi-
step synthesis of hexofuranoside-containing bioactive targets. Thus,
galactose was converted to anomeric methyl furanosides 12 via this ferric
 
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