Environmental Engineering Reference
In-Depth Information
Table 2
Applied speciation steps for organotin determination in marine sediment reported in papers published since 2000
Extraction
Derivatization
Preconcentration
Analysis
•
leaching with organic polar
•
hydride generation [28]
•
SPME [12, 29],
•
GC-MIP-AES [41]
[14, 15, 26-36, 44]
•
organoborate:
[31, 34, 36, 39, 49]
•
GC-ICP-AES [39]
and non-polar solvents
- ethylation [14, 15],
•
cryogenictrap [23]
•
GC-ICP-MS [14, 15, 26, 33, 44]
[18, 21, 22, 44, 47]
[18, 26, 29, 31, 33],
•
pervaporation [50]
•
HPLC-ICP-MS [27, 43]
+ complexing agents using
[36-39, 41, 44, 47]
•
GC-AAS [28, 35]
MW [15, 26, 43],
- propylation [34]
•
GC-ICPMS [23]
•
•
US [15, 26, 29, 31-36, 40, 41, 44, 48],
Grignard:
GC-MS [18, 29, 30, 32-34, 40],
ASE [14, 27],
- ethylation [42]
•
GC-PFPD [37, 48, 50]
MS [18, 26, 37-39, 41]
- propylation [21]
•
GC-FPD [21, 38, 47]
•
SPE [35, 40]
- pentylation [30, 32, 48]
•
MS [22]
•
GC-FID [31, 36]
GC-MS
/
