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(a) In-situ agglomerated material
(b) Hard sintered agglomorates
Figure 15. Agglomerated material after Coal-Vinasse co-firing.
(a) Deposits on feed pipe
(b) Deposits on gas analysis probe
Figure 16. Sticky deposits on the gas analysis probe and feed pipe.
Table 24. SEM analysis of Coal-Vinasse Agglomeration test
Site of interest 1
Site of interest 2
Element
Weight (%)
Atomic (%)
Weight (%)
Atomic (%)
O
48.29
62.23
40.98
60.40
F
4.64
5.03
-1.76
-2.18
Na
3.46
3.1
3.37
3.46
Mg
0.3
0.26
0.4
0.39
Al
1.35
1.03
2.13
1.86
Si
28.37
20.83
23.48
19.71
P
0.26
0.18
0.23
0.17
S
2.85
1.83
3.33
2.45
K
9.84
5.19
10.22
6.16
Ca
0.63
0.32
0.82
0.48
Fe
-
-
16.8
7.09
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