Digital Signal Processing Reference
In-Depth Information
Error Analysis in FPT (−) via Shape Spectra (Component & Total: Left, Residual: Right); FID Length: N P =180,220,260
Absorption Component and Total Shape Spectra
Residual Spectrum: Subtraction of 2 Total Shape Spectra
18
12
PADE: FPT (−)
B 0 =1.5T
N P = 180
N P = 180
8
N P = 180, 220
B 0 =1.5T
14
5+6+7
Converged (total only)
4
Converged
14+15
10
0
16+17
8
22+23
9
6
−4
10
21
19
12
20
1+2
3+4
18
13
FPT (−) (220) − FPT (−) (180)
−8
25
24
2
0
−12
5
4
3
2
1
5
4
3
2
1
(i) Chemical shift (ppm)
(iv) Chemical shift (ppm)
Absorption Component and Total Shape Spectra
Residual Spectrum: Subtraction of 2 Total Shape Spectra
18
12
PADE: FPT (−)
B 0 =1.5T
8
N P = 220
N P = 220
N P = 220, 260
B 0 =1.5T
14
5+6+7
Converged (both)
4
Converged
14+15
10
0
16+17
8
22+23
9
6
−4
10
21
19
11+12
20
1+2
3+4
18
13
FPT (−) (260) − FPT (−) (220)
−8
25
24
2
0
−12
5
4
3
2
1
5
4
3
2
1
(ii) Chemical shift (ppm)
(v) Chemical shift (ppm)
Absorption Component and Total Shape Spectra
Residual Spectrum: Subtraction of 2 Total Shape Spectra
18
12
PADE: FPT (−)
B 0 =1.5T
8
N P = 260
N P = 260
N P = 180, 260
B 0 =1.5T
14
5+6+7
Converged (both)
4
Converged
14+15
10
0
16+17
8
22+23
9
6
−4
10
21
19
11+12
20
1+2
3+4
13
FPT (−) (260) − FPT (−) (180)
18
−8
25
24
2
0
−12
5
4
3
2
1
5
4
3
2
1
(iii) Chemical shift (ppm)
(vi) Chemical shift (ppm)
FIGURE 3.12
Left: absorption total shape spectra superimposed on top of the correspond
ing component shape spectra in the FPT (−) near full convergence for signal
lengths N P = 180, 220, 260. Right: Consecutive difference spectra for absorp
tion total shape spectra in the FPT (−)
for signal lengths N P = 180, 220, 260.
 
Search WWH ::




Custom Search