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Br
Br
(0.2 mmol)
Br
H
NH
2
7.29
7.27
P
t
Bu
3
Br
(0.03 mmol)
K
2
CO
3
(0.4 mmol)
H
Pd
Pd(P
t
Bu
3
)
2
H
C
6
D
6
, rt, 3 d
7.29
100
°
C, 14 h
Br
(0.01 mmol)
77%
7.30a
(0.177 mmol)
Scheme 7.20 Testing the catalytic activity of complex 7.30a.
Adapted from Ref. 83. Copyright 2010 American Chemical Society.
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