Pesticide Residues in Mother’s Milk - Pesticides: Evaluation of Environmental Pollution - page 550

TABLE 17.3
The Standard Method Consists of Three Steps: Extraction, Cleanup, and Estimation of Organochlorine Pesticides in Mother's Milk

Extraction
Solvents

Cleanup
Methods

Determination
Methods References References References

Acetone: Hexane Burke et al. (2003), Mueller

et al. (2008), and Raab et al.
(2008)

Florisil Saeed et al. (2000), Bates et al.

(2002), Kunisue et al. (2004b),
Kumar et al. (2006a),
Ennaceur et al. (2007), Sharaf
et al. (2008) and Devanathan
et al. (2009)

Electron capture
detector

Burke et al. (2003), Kumar et al. (2006a),
Johnson-Restrepo et al. (2007), Subramanian
et al. (2007), Malarvannan et al. (2008),
Okonkwo et al. (2008), Alle et al. (2009),
Behrooz, et al. (2009), Devanathan et al.
(2009), Waliszewski et al. (2009), Cok et al.
(2011), and Tutu et al. (2011)

Hexane:
Acetonitrile:
Ethanol

Ennaceur et al. (2007) Florisil-Silica

Gel column

Yu et al. (2007) Mass spectrometry Wong et al. (2002), Burke et al. (2003), Minh

et al. (2004), Poon et al. (2005), Hui et al.
(2008), Mueller et al. (2008), Haraguchi et al.
(2009), Zhou et al. (2011), Srivastava et al.
(2011) and Fujii et al. (2011)

Hexane Rodas-Ortíz et al. (2008) Silica Tutu et al. (2011) High-resolution

mass spectrometry

Saleh et al. (2002), Gonzalez-Rodriguez et al.
(2005), and Mueller et al. (2008)

Ethanol Yu et al. (2007) GPC Sudaryanto et al. (2005),

Kunisue et al. (2006),
Subramanian et al. (2007),
Raab et al. (2008), Hui et al.
(2008), Devanathan et al.
(2009), Zhou et al. (2011),
and Fujii et al. (2011)

Bench-topped
double focusing
mass selective
detector

Sudaryanto et al. (2005)

Ethanol/toluene Hui et al. (2008) — — Selective ion

monitoring mode

Bates et al. (2002)

Dichloromethane Kumar et al. (2006a) — — Fourier transform

infrared (FTIR)

Srivastava et al. (2011)

Ethyl acetate:
methanol:
acetone

Schinas et al. (2000) — — — —

Formic acid and
sulfuric acid

Covaci et al. (2001), Rodas-
Ortíz et al. (2008), Behrooz
et al. (2009) and Waliszewski
et al. (2009)

— — — —