Pesticide Residues in Surface Water and Groundwater - Pesticides: Evaluation of Environmental Pollution - page 281

12, carbamates +
their degradation
products

SPE (Bond Elut Jr.
C18)

X-Terra (250 × 4.6 mm i.d.
and 5 μm particle size)

El Atrache
et al. (2005)

TPs of 4 triazines Spiked

SW

Direct injection X-Terra C18 (250 × 2.1 mm

i.d. and 5 μm particle size)

Water (0.01% HCOOH),
MeOH (0.01% HCOOH )

ESI-Q-
TOF

— Ibáñez et al.

(2004)

15, multiclass +
metabolites

SW SPE (Oasis HLB) Nucleodur C18 gravity

(125 × 2 mm i.d. and 3 μm
particle size)
For acidic pesticides:
Gromsil C18 (150 × 2 mm,
3 μm)

Water (0.1% HCOOH),
MeOH (0.1% HCOOH)
(for acidic pesticides
0.6 % HCOOH)

ESI-QqQ 0.15-3 Gomides

Freitas et al.
(2004)

47, multiclass + TPs On-line SPE

(PRP-1)

Kromasil C18 (125 × 2.0 mm
i.d. and 5 μm particle size)

Water (0.01% HCOOH),
ACN (0.01%
HCOOH)

ESI-QqQ
ESI-Q-
TOF

— Hernández

et al. (2004)

31, multiclass +
some metabolites

WW, DW Direct injection Zorbax Eclipse XDB-C18

(50 × 4.6 mm i.d. and 1.8 μm
particle size)

Water - MeOH (5 mM
ammonium formate)

ESI-QqQ 2-15 Díaz et al.

(2008)

20, multiclass SW, GW On-line SPE

(PLRP-s) for
acidic pesticides:
(Hysphere Resin
GP)

Purospher STAR-RP-18e
(125 × 2 mm i.d. and 5 μm
particle size)

Water - ACN ESI-QqQ 0.004-2.8 Kampioti et al.

(2005)

5, triazines and
phenylureas

SW, GW,
DW

SPE (LiChrolut
RP-18)

LiChrospher 100 RP-18
(250 × 4 mm i.d. and 5 μm
particle size)

Water, ACN APCI-Q 1.61-

10.95

Frías et al.
(2004)

SW, surface water; GW, groundwater; WW, wastewater; DW, drinking water; CAN, acetotnitrile; HAc, acetic acid; MeOH, methanol; HCOOH, formic acid; NH 4 Ac,
ammonium acetate; TIS, turbo ion spray.