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In-Depth Information
OAc
AcO
O
N 3
OAc
O
12 h rt,
1 h 80 °C,
MW (20 W)
O
AcO
O
N
AcO
N
N
N
120
AcO
N
N
119
O
AcO
O
AcO
AcO
AcO
OAc
O
O
N 3
OAc
O
AcO
O
N
N
N
AcO
N
AcO
N
N
121
122
O
AcO
O
AcO
AcO
OAc OAc
AcO
O
N 3
O
N
O
N
AcO
N
AcO
N
124
AcO
N
O
N
O
AcO
OAc
123
O
OAc
OAc
AcO
AcO
O
N 3
AcO
O
OO
AcO
N
N
N
N
AcO
N N
126
AcO
125
O O
OAc
AcO
OAc
AcO
AcO
N 3
AcO
O
O
O
N
AcO
N
128
AcO
N
N
N
N
O
127
O
AcO
AcO
O
AcO
OAc
OAc
N 3
AcO
OAc
O
O
OAc
O
AcO
N
N
130
O
N
N
129
N N
OAc
O
O
AcO
AcO
OAc
OAc
N 3
AcO
OAc
O
O
OAc
AcO
O
132
N
O
131
N N
OAc
N
O
N N
O
AcO
AcO
SCHEME 5.28
Microwave-assisted
synthesis
of
macrocycles
from
bifunctionalized
monosaccharides.
 
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