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BnO
P
O
O
O
BnO
O
O
O
O
NH
BnO O
O
O
H
O
O
NH
O
O
O
BnO
O
BnO
COOH
OH
26
OH
H
N
O
O
Ph
OH
HO
OH
HO
O
HO
O
O
O
O
OH
N 3
OH
O
OH
27
BnO
P
O
DIEA, CuI, THF, MeOH, rt, 24h
BnO
O
O
O
COOH
BnO
OH
O
O
NH
O
BnO O
OH
O
N
O
OH
O
HO
O
HO
H
O
O
NH
O
O
O
O
Ph
O
N
OH
HO
O
O
N N
O
OH
OH
BnO
O
OH
BnO
28
FIGURE 4.7
Synthesis and functionalization of an alkynyl-Lipid A analog.
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