Civil Engineering Reference
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Ultracentrifugation time
3.7 Schematic fi gure showing the progression of the sedimentation of
nano-materials inside a tube during ultracentrifugation (Metaxa et al. ,
2012).
(a)
(b)
(c)
￿ ￿ ￿ ￿ ￿ ￿
3.8 Suspensions of carbon nanotubes ultracentrifuged for (a) 30 min,
(b) 45 min and (c) 60 min (Metaxa et al. , 2012).
tion quantity, A , is measured by the particle size. The agglomeration per-
centage is critical because, in certain cases, dispersion between two images
can be identical, although the agglomeration percentage will have changed.
In both cases, a quantifi able percentage is calculated based on the statistical
probability that either the free-path spacing or particle size will fall within
a certain percentage above and below l , where l is either the mean spacing
or the particle size. A high value of D indicates a better dispersion. A lower
value of A indicates a reduction in agglomeration.
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