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O
O
O
O
N
N
O
NaHCO
3
(1.5 equiv)
BocHN
BocHN
+
H
OMe
HCl·H
2
N
OMe
Vibrating ball-mill, 30 Hz, 1 h
O
O
O
Boc-Val-NCA
HCl·H-Ala-Gly-OMe
Boc-Val-Ala-Gly-OMe
89%
Scheme 6.14 Mechanosynthesis of the tripeptide Boc-Val-Ala-Gly-OMe.
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